Wildcat Discovery Technologies

Putting a stored liquid-handling robot to work

Mechanical Engineer · 2011–2013

While technicians spent hours mixing experimental battery solutions by hand, Wildcat had a liquid-handling robot sitting unused in storage. Rather than buying new equipment, I adapted the stored machine for solution synthesis—reusing its motion gantry and liquid-transfer hardware to prepare chemical mixtures automatically.

Once that setup was running daily mixture prep in the lab, it also gave us a practical way to test automated battery-slurry coating, where accurate dispensing alone did not guarantee an even film across the target area.

Automated liquid-handling XY gantry and four-channel pipetting manifold poised over a custom-machined aluminum sample-vial block.Enlarge imageEnlarge: Automated liquid-handling XY gantry and four-channel pipetting manifold poised over a custom-machined aluminum sample-vial block.
Adapted liquid-handling gantry dispensing programmed chemical mixtures into custom sample-vessel holders on the laboratory deck. Illustrative image.

Letting technicians specify the mixture

The stored robot already handled movement and pipetting reliably; making it useful on the floor meant fitting it to our containers and giving technicians simple controls. I designed custom sample holders around the lab’s vessels and built a LabVIEW interface where technicians entered their target mixture ratios and started a run—turning an idle machine from storage into a daily lab tool.

1. XY DISPENSE ARRAY (12-VIAL FIXTURE) X-axis rail A1 A2 A3 A4 B1 B2 B3 B4 C1 C2 C3 C4 Y-arm pipette Programmed ratios dispensed across 12 vials per cycle 2. SUBSTRATE WETTING & SPREAD GEOMETRY UNASSISTED DISPENSE (HIGH CONTACT ANGLE) Beaded drop Cross-section Incomplete edge coverage SURFACE TREATMENT + HEAT + VIBRATION Uniform thin film Heated + vibrated stage Full target area wetted Controlled spreading across target electrode area
Automated liquid-handling dispense array and substrate wetting geometry for high-throughput battery-material preparation.

Getting slurry to cover the intended area

Once solution mixing was running, I tested whether the robot could also coat sample substrates with battery slurry. Slurry had to wet and spread evenly across the metal cup without running past its edges—simply dispensing the right volume in the center often left partially wetted cells with bare metal along the rim.

To test surface prep repeatably, I built a motorized dual-torch flame-treatment stage to pass substrates under controlled heat before deposition, and evaluated it alongside plasma treatment and mechanical vibration to see how each improved wetting and edge coverage. That study gave the team a clear picture of what surface treatment and vibration could solve—and where thicker slurries required dedicated coating equipment rather than a modified liquid handler.

Partially wetted coin-cell cup after dispensing alone, where dark battery slurry beaded up and pulled away from the metal edges.Enlarge imageEnlarge: Partially wetted coin-cell cup after dispensing alone, where dark battery slurry beaded up and pulled away from the metal edges.
Partially wetted coin-cell cup after dispensing alone: dark battery slurry beaded up and pulled away from the metal edges instead of covering the full target area.
Prototype flame-treatment stage built to treat substrates before deposition, showing dual propane torches over a machined manifold driven by a Vexta stepper stage and Arduino controller.Enlarge imageEnlarge: Prototype flame-treatment stage built to treat substrates before deposition, showing dual propane torches over a machined manifold driven by a Vexta stepper stage and Arduino controller.
Prototype flame-treatment stage built to treat substrates before deposition: dual propane torches over a machined manifold, driven at repeatable speeds by a Vexta stepper stage and Arduino controller.

Experience used here

Laboratory automation · Custom robot tooling · LabVIEW · Liquid handling · Process development · Equipment adaptation

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